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Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.

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However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur. This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility. Learn more about our laboratories – where they are located; the unique capabilities they have and how they can awtm you solve your technical and commercial challenges.

See Appendix X1 atm information regarding test selection. A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use. It does not say what to do about duplex or super austenitic alloys.

Intergranular Corrosion Testing: An Overview of ASTM A262

The effect of post weld surface treatments on the corrosion resistance of super duplex stainless steel welds in sea water Work Item s – proposed revisions of this standard. Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack. The test methods in Table 1 were designed with specific alloys in mind, but the proliferation of new CRAs has meant that the selection of a suitable test method is difficult.

Where a standard is included in a purchase specification, this must be followed, although it is advised that unsuitable tests, such as the Huey test for asttm and super austenitic stainless steels, are queried. Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys. The samples are etched after metallographic preparation for cross-sectional examination which is thoroughly viewed with a traverse from inside to outside diameters of rods and tubes, from face to face on plates, and across all zones such as weld metal, weld-affected zones, and base plates on specimens containing welds.


SEP does not require ageing, although it might be required in a specification calling up this standard. Vickers A62 5Kg and 10Kg.

ASTM A was designed for austenitic stainless steels, specifically the series alloys. Contact us by Phone a26 Email to find out how we can help your industry. Selection of a Test Method The test methods in Table 1 were designed with specific alloys in mind, but the proliferation of new CRAs has meant that the selection of a suitable test method is difficult.

The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb q262 Ti, or the effectiveness of reducing carbon content to resist intergranular attack. Based on your materials, application, and asttm, the other 4 methods provide specific focuses. Make an Enquiry Notice: ASTM G28 does not require samples to be heat treated. The test solutions and exposures for some common intergranular corrosion tests.

Intergranular simply means that the corrosion is taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA.

SEP also gives guidance on which of its methods apply to which alloys: It is the satm of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.

The etch structure types used to classify the specimens are: JavaScript is required for this content. The first and fastest step is the ASTM A Practice A, a aetm same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion.

The oxalic acid test is commonly awtm before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.


Intergranular Corrosion Tests for CRAs

These tests were introduced when the carbon content in CRAs typically hit 0. Suggested test methods for different corrosion resistant alloys. Contact us now for pricing or a quote! Please refer to the specification for more details.

This abstract is a brief summary of the referenced standard.

Please share this page: Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. This means that carbide formation during welding is highly unlikely, and modern CRAs should easily pass one of these tests.

Typical examination magnification is X to X. Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required.

None of these are identical and cross substitution of results is not possible. Practice B, also known as the Streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance. Discover perspectives, resources, and advice from our world-leading Engaged Experts. It can be seen that some alloys fall a22 two categories, and no guidelines are given for selecting the most appropriate.

Technical Resources

This specification is for detecting susceptibility to intergranular attack IGA. R Baboian, Corrosion Tests and Standards: The Huey test method C is only for molybdenum-free grades, such as L, as alloys with molybdenum show high rates of attack in this test. Some suggested criteria for the listed alloys are shown in Table 2, below. The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack.

What is your typical turnaround time? The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:. In everyday applications, corrosion varies by materials and solutions.

This document also points out which alloys the tests are intended for, and recommends the most appropriate test when none w262 specified.